STICKY RICE SLURRY-MODIFIED LIME-METAKAOLIN STABILIZATION OF SILTY CLAY: MECHANICAL PERFORMANCE AND MICROSTRUCTURAL CHARACTERIZATION

Authors

  • Tao Jiang (Corresponding Author) School of Civil Engineering and Architecture, Hubei Polytechnic University, Huangshi 435003, Hubei, China.
  • ChunLong Liu Pingyang County Transportation Bureau, Wenzhou 325400, Zhejiang, China. Institute of Geotechnical Engineering, Xi’an University of Technology, Xi’an 710048, Shaanxi, China.
  • ZhiQiang Zhang Institute of Geotechnical Engineering, Xi’an University of Technology, Xi’an 710048, Shaanxi, China.

Keywords:

Sticky rice slurry, Metakaolin, Lime, Silty clay, Unconfined compressive strength, Microstructure

Abstract

Lime-stabilized silty clays are widely used in subgrade construction and earthen heritage conservation, but their relatively slow strength development, susceptibility to wet-dry deterioration and limited long-term durability still constrain their broader engineering applications. In this study, a ternary binder consisting of sticky rice (SR) slurry, metakaolin (MK) and hydrated lime was formulated to stabilize a low-plasticity silty clay, with the aim of exploiting both the pozzolanic reactivity of calcined kaolin and the biomolecular templating effect of amylopectin. A systematic series of unconfined compressive strength (UCS) tests was conducted on lime-soil (LS), metakaolin-lime-soil (ML) and sticky rice-metakaolin-lime-soil (SM) specimens with varying lime contents, metakaolin dosages, sticky rice concentrations and water-to-solid ratios, cured for 7, 28 and 90 days. The microstructural and mineralogical evolution of the stabilized matrix was characterized using scanning electron microscopy (SEM) and X-ray diffraction (XRD), and the internal water retention behavior was tracked throughout the curing period. The experimental results indicate that the optimum binder composition corresponds to 13% lime, 10% metakaolin and 3% sticky rice at a water-to-solid ratio of approximately 0.34, beyond which strength either plateaus or declines because of dilution or excess organic phase. Compared with conventional LS and ML systems, the SM specimens develop a denser and more homogeneous gel-rich microstructure, exhibit a more pronounced consumption of portlandite and a stronger amorphous hump associated with C-S-H and C-A-H, and retain internal moisture more effectively during curing. The synergetic interaction between the biopolymer network of sticky rice and the pozzolanic products of the lime-metakaolin system is identified as the principal mechanism underlying the strength enhancement, providing a sustainable and historically inspired stabilization route for silty clay.

References

[1] Shi Y, Li S, Zhang T, et al. Compaction and shear performance of lime-modified high moisture content silty clay. Case Studies in Construction Materials, 2024, 21: e03529. DOI: 10.1016/j.cscm.2024.e03529.

[2] Li X M, Wu D, Yin S, et al. Natural hydraulic lime versus lime-metakaolin modified silt in earthen heritages. Materials and Structures, 2022, 55(7).

[3] Brzyski P, Cieślikiewiczet Ł, Pietrak K, et al. The combined effect of gum arabic and casein on selected parameters of lime-metakaolin paste and hemp concrete for use as wall material. Journal of Building Engineering, 2026, 123: 115824. DOI: 10.1016/j.jobe.2026.115824.

[4] Ryou J E, Jang C, Gang S, et al. A review of biopolymers in geotechnical engineering: Mechanical properties, dynamic behavior, applications, and mechanisms. Journal of Rock Mechanics and Geotechnical Engineering, 2026, 18(6): 4971-4997.

[5] Razali R, Rashid ASA, Lat DC, et al. Shear strength and durability against wetting and drying cycles of lime-stabilised laterite soil as subgrade. Physics and Chemistry of the Earth, Parts A/B/C, 2023, 132: 103479. DOI: 10.1016/j.pce.2023.103479.

[6] Hassannezhad K, Akyol Y, Dursun M C, et al. Effect of Metakaolin and Lime on Strength Development of Blended Cement Paste. Construction Materials, 2022, 2(4): 297-313.

[7] Li X, Zhang H, Guo Y, et al. Effect of Dry‐Wet Cycles on Strength Properties and Microstructure of Lime‐Metakaolin‐Modified Soil. Advances in Civil Engineering, 2022: 1296288. DOI: 10.1155/2022/1296288.

[8] Onyelowe K C, Ebid A M, Kontoni DPN, et al. Effect of Metakaolin and Ashcrete blend on the mechanical properties of lateritic soil for sustainable subgrade and subbase construction. Multiscale and Multidisciplinary Modeling, Experiments and Design, 2023, 7(2): 1197-1208.

[9] Luo Y, Meng J, Wang D, et al. Experimental study on mechanical properties and microstructure of metakaolin based geopolymer stabilized silty clay. Construction and Building Materials, 2022, 316: 125662. DOI: 10.1016/j.conbuildmat.2021.125662.

[10] Anburuvel A. The Engineering Behind Soil Stabilization with Additives: A State-of-the-Art Review. Geotechnical and Geological Engineering, 2023, 42(1): 1-42.

[11] Greco P F, Pepi C, Gioffré M. A novel biocomposite material for sustainable constructions: Metakaolin lime mortar and Spanish broom fibers. Journal of Building Engineering, 2024: 83.

[12] Fan W, Chen W, Zhang Q, et al. Feasibility of protecting earthen sites with sticky rice and lime composite. Construction and Building Materials, 2022, 346: 128449. DOI: 10.1016/j.conbuildmat.2022.128449.

[13] Pant R, Zhang G. Nanomechanical and microstructural characterization of a hybrid clay-lime-starch composite, in Geo-Congress 2014. ASCE Library: Shanghai, 2014: 2849-2857.

[14] Ullah S, Hegarty B, Yu X. An Effective Strategy to Preserve the Durability of Biopolymer Soil Treatment. Biogeotechnics, 2026. DOI: 10.1016/j.bgtech.2026.100232.

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Published

2026-07-06

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Section

Research Article

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How to Cite

Tao Jiang, ChunLong Liu, ZhiQiang Zhang. Sticky Rice Slurry-Modified Lime-Metakaolin Stabilization Of Silty Clay: Mechanical Performance And Microstructural Characterization. World Journal of Engineering Research. 2026, 4(5): 45-52. DOI: https://doi.org/10.61784/wjer3117.